
Scanning Electron Microscopy with Polarization Analysis
[EPG Pub# 555] is a technique that we have
developed for looking at very small magnetic structures.
SEMPA images the magnetization by measuring the spin polarization of secondary
electrons emitted in a scanning electron microscope. The secondary electron
spin polarization is directly related to the magnetization of the sample. SEMPA
therefore produces a direct image of the magnitude and the direction of the
magnetization in the region probed by the incident electron beam.
SEMPA has several unique capabilities that set it apart from other magnetic
imaging techniques: First, unlike most other techniques which image the
magnetic field, SEMPA measures the magnitude and direction of the magnetization
directly. Second, SEMPA has the high spatial resolution (about 10 nm),
long working distance, and large depth of field characteristic of scanning
electron microscopes. Third, SEMPA measurements of the magnetization are
intrinsically independent of the topography, but the magnetic and topographic
maps are measured simultaneously. This feature allows investigations of the
correlations between magnetic and topographic structures. And finally, SEMPA is
a relatively surface sensitive technique, because of the small (~1 nm)
secondary electron escape depth. This makes SEMPA especially well suited for in
situ studies of thin film and surface magnetization.
Currently, two SEMPA instruments are available in the Electron Physics Group.
Both are also scanning Auger microprobes which allow us to obtain compositional
maps of specimens as well as SEMPA images. Both instruments also use the same
compact electron spin polarization analyzers [EPG Pub# 513] that were developed at NIST.
One apparatus (a JEOL JAMP-30) has 60 nm spatial SEMPA resolution and has
been modified with the addition of thin film evaporators and a Reflection High
Energy Electron Diffraction (RHEED) system in order to do in situ measurements
of thin film and multilayer magnetism.
The other SEMPA apparatus (a PHI 670) has a high brightness field emission
cathode which enables it to image magnetic microstructures with 10 nm
spatial resolution.
Online: August 1995
Last Updated: July 2007